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1 H NMR (400 MHz, DMSO-d 6 ) : δ ppm 8.70 (d, J = 9.2 Hz, 1H), 7.66 (d, J = 9.6 Hz, 1H), 7.59–7.53 (m, 2H), 7.49–7.46 (m, 1H), 7.21–7.16 (m, 4H), 5.01–4.98 (m, 1H), 4.71–4.68 (m, 1H), 4.32–4.28 (m, 1H), 3.89–3.42 (m, 5H), 3.28–3.18 (m, 4H), 2.98–2.94 (m, 1H), 2.63–2.61 (m, 1H), 1.45 (s, 9H), 1.35–1.33 (m, 2H), 1.16–1.14 (m, 2H) LCMS (ES, m/z) calculated for C 32 H 37 N 6 O 3 + [(M + H) + ] 553.2, observed 553.2

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